Journal
ORGANIC PROCESS RESEARCH & DEVELOPMENT
Volume 21, Issue 7, Pages 987-991Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.oprd.7b00101
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- [0R00001809]
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After successful synthesis of hexabenzylhexaazaisowurtzitane (HBIW) on a laboratory scale (0.25 L reactor), it was performed on a multilaboratory scale (10 L reactor) and subsequently in an experimental installation in which a 300 L reactor was built. Seven syntheses were carried out in the unit on a pilot scale to produce 250 kg of HBIW. The pilot-scale syntheses ran with a yield comparable to those observed for the processes conducted on a large-laboratory scale. Some modifications were suggested that allowed for reduction of the HBIW weight unit by approximately 50%.
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