Journal
ORGANIC LETTERS
Volume 19, Issue 12, Pages 3055-3058Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.7b01073
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- NSF under CCI Center [CHE-1205646]
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A tandem reaction system has been developed for the preparation of donor/acceptor-substituted diazo compounds in continuous flow coupled to dirhodium-catalyzed C-H functionalization or cyclopropanation. Hydrazones were oxidized in flow by solid-supported N-iodo-p-toluenesulfonamide potassium salt (PS-SO2NIK) to generate the diazo compounds, which were then purified by passing through a column of molecular sieves/sodium thiosulfate.
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