Journal
ORGANIC LETTERS
Volume 19, Issue 7, Pages 1828-1830Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.7b00591
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Funding
- Tsinghua University
- 1000 Talents Recruitment Program
- National Natural Science Foundation of China [21672123]
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The first total synthesis of the opened-type Kopsia alkaloid grandilodine B is reported. Four stereocenters of this alkaloid, three of them quaternary, are stereoselectively generated by a Diels-Alder reaction, a diastereoselective cyanation of tertiary alcohol, and a facial selective nitrone 1,3-dipolar cycloaddition.
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