Journal
ORGANIC LETTERS
Volume 19, Issue 16, Pages 4227-4230Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.7b01867
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Funding
- NIH NIGMS [R01 GM120205]
- NSF
- National Science Foundation [CHE-0619638]
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Protocols for the synthesis of diverse pentacarboxycyclopentadienes are described. Starting from readily available pentacarbomethoxycyclopentadiene, transesterification offers single-step access to aliphatic ester derivatives, while treatment with amines produces mono- or diamides. For less nucleophilic alcohols, an alternative procedure involving the in situ generation and esterification of a putative cyclopentadiene pentaacid chloride has been developed.
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