Journal
ORGANIC LETTERS
Volume 19, Issue 13, Pages 3640-3643Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.7b01642
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Funding
- National Natural Science Foundation of China [21425415, 21274058]
- National Basic Research Program of China [2015CB856303, 2011CB935801]
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An efficient Rh(III)-catalyzed C-H activation protocol has been developed for the synthesis of 2,3-benzodiazepines with use of N-Boc hydrazones and diazoketoesters as substrates. The reaction features retention of the C = N and N-N bonds and selective cleavage of the N-Boc moiety.
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