Journal
ORGANIC LETTERS
Volume 19, Issue 9, Pages 2358-2361Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.7b00894
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Funding
- NSFC [21172034, 21372039, 21372038, 21522202]
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An ambient-light-promoted and,metal-free three-component reaction of active methylene compounds perfluoroalkyl iodides, and guanidines/amidines is reported: This constitutes a powerful method to prepare prfluoroalky-lated pyrinudines with mild reaction Conditions, broad substrate scope, excellent functional group tolerance, and simple operation. A radical/polar mechanism involving the formation of a halogen-bond adduct and radical cross-coupling is proposed.
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