Journal
ORGANIC LETTERS
Volume 19, Issue 7, Pages 1626-1629Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.7b00435
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Funding
- EPSRC [EP/K503885/1]
- Leverhulme Trust [RPG-2015-088]
- Newcastle University
- Engineering and Physical Sciences Research Council [EP/K503885/1] Funding Source: researchfish
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Tin(IV) catalysis allows isolation of a boron dipyrroirrethene derivative bearing a solitary strap around the boron center. The conditions favor internal cyclization without contamination by side products and provide high yields of product in good purity. A phenolate-based strap imposes chirality and causes geometrical distortion of the dipyrrin. Relatively-strong fluorescence is observed for single crystals, evaporated films, and adsorbed layers. Single-Crystal absorption and emission spectra resemble those observed from-solution with contributions froth a dimer.
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