Journal
ORGANIC LETTERS
Volume 19, Issue 24, Pages 6666-6669Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.7b03392
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Funding
- NSFC [21632003, 21372105, 21572087]
- 111 program from the MOE of P. R. China
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A 3,4,5-trimethylphenol and Lewis acid dual catalyzed cascade reaction of donor acceptor (D-A) cyclopropanes via ring-opening and cyclization is developed. In this reaction, a phenolic compound was used as a covalent catalyst for the first time. Additionally, control experiments proved that 3,4,5-trimethylphenol completed the catalytic cycle by accomplishing the C-C bond cleavage. Using this strategy, a wide variety of substituted naphthalenes has been synthesized from D-A cyclopropanes moderate to high yields under mild conditions.
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