Journal
ORGANIC LETTERS
Volume 19, Issue 16, Pages 4171-4174Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.7b01658
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Funding
- Ministry of Science and Technology, Taiwan [MOST 1052113-M-033-003]
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An efficient alpha-sialylation method for many primary hydroxyl acceptors that include 6-OH glycosides has been developed. 7,8-Di-O-picoloyl sialyl glycoside was used as the glycosyl donor, and alpha-glycoconjugation was controlled by using the 7,8-di-O-picoloyl moiety in CH2Cl2. The methodology was successfully applied to the total synthesis of ganglioside Hp-s1 possessing neuritogenic activity.
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