Journal
ORGANIC LETTERS
Volume 19, Issue 15, Pages 4146-4149Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.7b02053
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Funding
- Fondation pour le Developpement de la Chimie des Substances Naturelles et ses Applications (Academie des Sciences)
- INSA Rouen, Rouen University
- CNRS
- EFRD
- Labex SynOrg [ANR-11-LABX-0029]
- Region Normandie
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The first synthesis of the proposed structures of chaetoviridins A 1-4 has been achieved in 10 steps by controlling the syn- or anti-aldol side chain. The angular lactone has been regioselectively introduced by condensation of a chiral dioxin-4-one to cazisochromene. Comparison of the NMR and circular dichroism data of the synthesized and reported natural products led to the complete reassignment and renaming of the chaetoviridins.
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