Journal
ORGANIC LETTERS
Volume 19, Issue 24, Pages 6518-6521Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.orglett.7b03216
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Funding
- NSF [GOALI SusChEM 1566212]
- Novartis
- Direct For Mathematical & Physical Scien
- Division Of Chemistry [1566212] Funding Source: National Science Foundation
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An especially mild, safe, efficient, and environmentally responsible reduction of aromatic and heteroaromatic nitro-group-containing educts is reported that utilizes very inexpensive carbonyl iron powder (CIP), a highly active commercial grade of iron powder. These reductions are conducted in the presence of nanomicelles composed of TPGS-750-M in water, a recyclable aqueous micellar reaction medium. This new technology also shows broad scope and scalability and presents opportunities for multistep one-pot sequences involving this reducing agent.
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