Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 15, Issue 16, Pages 3418-3422Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c7ob00654c
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Funding
- National Natural Science Foundation of China [21573262]
- Natural Science Foundation of Jiangsu Province [BK20161259]
- MOE SAFEA [B13025]
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A transition-metal-free lithiation-borylation method has been developed to access a variety of 1,1-diboronate esters with a fully substituted benzylic center from readily available secondary benzylic N,N-diisopropyl carbamates. The method is applicable to scale-up synthesis of 1,1-diboron compounds. Furthermore, the current method is also applicable to synthesizing optically active 1,1-silylboronate esters.
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