Journal
ACS APPLIED NANO MATERIALS
Volume 1, Issue 10, Pages 5425-5429Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acsanm.8b01663
Keywords
sputtered nanocarbon film; anodic stripping voltammetry; zinc ion; Zn-complex-based probe; lipopolysaccharide
Funding
- Ministry of Education, Culture, Science, Sports and Technology of Japan [25288071]
- Grants-in-Aid for Scientific Research [25288071] Funding Source: KAKEN
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We report an electrochemical method for detecting low concentrations of lipopolysaccharide (LPS), based on amplified zinc (Zn) signals on a sputtered nanocarbon film electrode. The nanocarbon film electrode allowed us to detect Zn2+ ions at a lower concentration than a conventional glassy carbon electrode using anodic stripping voltammetry. This was due to the efficient accumulation and detection of Zn2+ ions with very low noise made possible by the ultraflat nanocarbon film surface. The amplified Zn signals from a newly synthesized Zn-complex-based probe were successfully used to detect LPS with low concentrations without employing conventional reagents.
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