Journal
ORGANIC CHEMISTRY FRONTIERS
Volume 6, Issue 1, Pages 94-98Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c8qo01144c
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Funding
- Nanjing Tech University [39837137, 39837101, 3827401739]
- National Natural Science Foundation of China [21372210, 21672198, 21801129]
- State Key Program of National Natural Science Foundation of China [21432009]
- Natural science research projects in Jiangsu higher education institutions [18KJB150018]
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An efficient and straightforward three-component reaction of enamides, aryldiazonium tetrafluoroborates, and 1,4-diazabicyclo[2.2.2]octane bis(sulfur dioxide) (DABSO) for the direct C(sp(2))-H arylsulfonylation of enamides has been developed. This Cu(OTf)(2)-mediated SO2 insertion reaction proceeds smoothly to afford a diverse range of -amidovinyl sulfones bearing manifold functional groups in moderate to excellent yields with high regio- and stereoselectivities.
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