Journal
CHEMICAL COMMUNICATIONS
Volume 55, Issue 3, Pages 397-400Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c8cc09049a
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Funding
- National Natural Science Foundation of China [NSFC 21472213]
- National Key Research and Development Program [2016YFA0200302]
- Croucher Foundation (Hong Kong)
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An excellent level of enantioselectivity in asymmetric sulfenylation of 4-substituted pyrazolones was achieved with chiral iminophosphorane as the organocatalyst under continuum solvation conditions (up to 99% ee). Importantly, this catalytic process features high efficiency with excellent enantioselectivities, easy separation of products, low catalytic loadings and scale-up to grams without loss of enantioselectivity.
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