Journal
MICROSCOPY AND MICROANALYSIS
Volume 23, Issue 4, Pages 741-750Publisher
CAMBRIDGE UNIV PRESS
DOI: 10.1017/S1431927617012314
Keywords
in situ; TEM/STEM; electrochemical cell; sample preparation; FIB
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Funding
- EPSRC PROMINENT programme [EP/1003290/1]
- US DOE, Office of Science, Office of Basic Energy Sciences in the Photon Science Division [DE-AC02-06CH11357]
- Electron Microscopy Center, in the Center for Nanoscale Materials, Nanoscience and Technology Division of ANL
- EPSRC [EP/J021229/1] Funding Source: UKRI
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The capability to perform liquid in situ transmission electron microscopy (TEM) experiments provides an unprecedented opportunity to examine the real-time processes of physical and chemical/electrochemical reactions during the interaction between metal surfaces and liquid environments. This work describes the requisite steps to make the technique fully analytical, from sample preparation, through modifications of the electrodes, characterization of electrolytes, and finally to electrochemical corrosion experiments comparing in situ TEM to conventional bulk cell and microcell configurations.
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