Journal
CHEMICAL COMMUNICATIONS
Volume 55, Issue 14, Pages 2031-2034Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c8cc10157d
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Funding
- National Science Foundation of China [21822103, 21820102003, 21772052, 21772053, 21572074]
- Program of Introducing Talents of Discipline to Universities of China (111 Program) [B17019]
- Natural Science Foundation of Hubei Province [2017AHB047]
- International Joint Research Center for Intelligent Biosensing Technology and Health
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A novel sequential reaction that combines a visible light-induced Wolff rearrangement of alpha-diazoketones and a Pd-catalyzed [3+2] cycloaddition of vinyl cyclopropanes with the resulting ketenes is described in this work. Selective O-allylic alkylation was observed over C-allylic alkylation, which unexpectedly led to a series of highly functionalized tetrahydrofurans with high efficiency (20 examples, 58-99% yields).
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