Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 17, Issue 7, Pages 1817-1821Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c8ob02756k
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Funding
- University of York
- BBSRC [BB/M012697/1]
- Royal Society [IE151281]
- BBSRC [BB/M012697/1] Funding Source: UKRI
- EPSRC [EP/P030653/1] Funding Source: UKRI
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Herein we report synthesis of complex heparan sulfate oligosaccharide precursors by automated glycan assembly using disaccharide donor building blocks. Rapid access to a hexasaccharide was achieved through iterative solid phase glycosylations on a photolabile resin using Glyconeer (TM), an automated oligosaccharide synthesiser, followed by photochemical cleavage and glycan purification using simple flash column chromatography.
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