Journal
CHEMICAL SCIENCE
Volume 10, Issue 11, Pages 3181-3185Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c9sc00100j
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Funding
- National Natural Science Foundation of China [21702113, U1504208, 21602119]
- China Postdoctoral Science Foundation
- Program for Science and Technology Innovation Talents in Universities of Henan Province [19HASTIT033]
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An electrochemical difluoromethylation triggered lactonization of alkenes was developed for the first time. This protocol employs readily prepared CF2HSO2Na as the difluoromethylating reagent, affording unprecedented CF2H-containing lactones in moderate yields. Moreover, with CF3SO2Na as the trifluoromethylating reagent, a wide array of CF3-containing lactones were obtained under additional supporting electrolyte- and catalyst-free conditions.
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