Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 17, Issue 13, Pages 3319-3323Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c9ob00373h
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Funding
- Soonchunhyang University Research Fund
- Basic Science Research Program through the National Research Foundation of Korea [NRF-2016-R1D1A1B03933723]
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Electrochemical oxidative radical trifluoromethylation/ semipinacol rearrangement sequences of alkenyl alcohols were developed in this study. This approach is environmentally benign and uses the shelf-stable Langlois reagent as a trifluoromethyl radical precursor and electrons as the oxidizing reagents. The present protocol offers a facile route to prepare beta-trifluoromethylated ketone derivatives.
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