Journal
CRYSTENGCOMM
Volume 21, Issue 13, Pages 2053-2057Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c8ce01720d
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Funding
- MEXT Japan
- Japan Society for the Promotion of Science (JSPS) KAKENHI [JP17K05745, JP18H04504]
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Herein, we report a new polymorph of amodiaquine dihydrochloride dihydrate obtained via heterogeneous crystallisation. This new polymorph exhibits similarity in molecular conformation as well as in its one-dimensional chain structure with a previously known polymorph, however with a difference in its two-dimensional sheet structure. Although crystal DFT-calculations predict the new form to be thermodynamically less stable compared to the previously known polymorph, the preparation method applied opened up the access to its metastable zone.
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