Journal
TURKISH JOURNAL OF CHEMISTRY
Volume 43, Issue 2, Pages 464-+Publisher
Tubitak Scientific & Technological Research Council Turkey
DOI: 10.3906/kim-1807-101
Keywords
Boric acid; microwave irradiation; solvent-free; green method; 2-amino-4,6-diarylnicotinonitrile
Funding
- Iran National Science Foundation
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Microwave irradiation has been used to improve the one-pot synthesis of substituted 2-amino-4,6-diarylnicotinonitrile in the presence of boric acid as an efficient and green catalyst under solvent-free conditions within 48-60 s. All the analogs that have not been reported previously were characterized by their melting points, IR, H-1 NMR, and C-13 NMR spectra. One of the structures was verified by the analysis of a single crystal. The reported synthetic procedure provided remarkable advantages such as short reaction times, excellent yield, facile workup, and the use of a green catalyst.
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