Journal
CHEMICAL COMMUNICATIONS
Volume 55, Issue 42, Pages 5958-5961Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c9cc02319d
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Funding
- SERB, India [ECR/2015/000600]
- IIT Roorkee [SMILE-32]
- IIT-R
- [DST/2018/IF180079]
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The first nickel- catalysed dehydrogenative coupling of primary alcohols and ethylene glycol with aromatic diamines for selective synthesis of mono- and di- substituted benzimidazoles and quinoxalines is reported. The earth- abundant, non- precious and simple NiCl2/ L1 system enables the synthesis of N- heterocycles releasing water and hydrogen gas as byproducts. Mechanistic studies involving deuterium labeling experiments and quantitative determination of hydrogen gas evaluation were performed.
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