4.7 Article

A laboratory-based double X-ray spectrometer for simultaneous X-ray emission and X-ray absorption studies

Journal

JOURNAL OF ANALYTICAL ATOMIC SPECTROMETRY
Volume 34, Issue 7, Pages 1409-1415

Publisher

ROYAL SOC CHEMISTRY
DOI: 10.1039/c9ja00159j

Keywords

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Funding

  1. Polish Ministry of Science and Higher Education [IdPII2015000164]
  2. National Science Centre, Poland (NCN) [2016/21/D/ST4/00378]

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X-ray spectroscopy studies are usually performed using synchrotron radiation sources, which offer bright, coherent, energy-tuneable and monochromatic light. However, the application of synchrotron-based Xray emission spectroscopy (XES) and X-ray absorption spectroscopy (XAS) is directly constrained by the limited, infrequent access to central facilities. With the advent of new technological solutions in the field of X-ray sources, optics and detectors, the development of efficient and compact laboratory X-ray spectroscopy systems is possible. A permanent laboratory-based setup offers the advantages of low cost and easy accessibility and, therefore, more flexibility in the preparation and scheduling of measurements. Herein, we report a laboratory X-ray setup allowing simultaneous XES and XAS measurements. The double von Hamos spectrometer performances are demonstrated by concurrent K beta XES and K-edge XAS measurements done for 3d elements.

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