4.7 Article

In-situ tensile tests under SEM and X-ray computed micro-tomography aimed at studying a self-healing matrix composite submitted to different thermomechanical cycles

Journal

JOURNAL OF THE EUROPEAN CERAMIC SOCIETY
Volume 37, Issue 10, Pages 3471-3474

Publisher

ELSEVIER SCI LTD
DOI: 10.1016/j.jeurceramsoc.2017.03.067

Keywords

Tomography; In situ tensile tests; Oxidation; Ceramic matrix composites; Self-healing behaviour

Funding

  1. Centre National de la Recherche Scientifique (CNRS)
  2. Safran Ceramics (SAFRAN GROUP)

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Ceramic matrix composite (CMC) based on SiC fibres and matrix is gradually introduced in aeronautical application, mostly in hottest parts of engines. Three dimensional (3D) structured materials are good candidates for complex parts such as turbine blades. Material is submitted to mechanical stresses at high temperatures in oxidizing and corrosive environments for long durations. During thermomechanical cycles, damage, oxidation and healing-phenomenon occur and develop in the material. X-ray computed micro-tomography (mu CT) and tensile test under scanning electron microscopy (SEM) are experimental means to study these phenomenons. These techniques are implemented for the understanding of the behaviour of the oxide (solid or liquid) in the crack of the material. The influence of the oxide in the crack was analyzed during tensile test under SEM or mu CT. The observation allows to determine the influence of the oxide on the reclosure of the crack during the unloading. (C) 2017 Elsevier Ltd. All rights reserved.

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