Journal
JOURNAL OF THE EUROPEAN CERAMIC SOCIETY
Volume 37, Issue 8, Pages 3009-3014Publisher
ELSEVIER SCI LTD
DOI: 10.1016/j.jeurceramsoc.2017.02.052
Keywords
High-temperature strength; Tantalum diboride; Boron suboxide; Elevated temperature fracture toughness
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Funding
- Grants-in-Aid for Scientific Research [15H04163] Funding Source: KAKEN
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Tantalum diboride - boron suboxide ceramic composites were densified by spark plasma sintering at 1900 C-omicron. Strength and fracture toughness of these bulk composites at room temperature were 490 MPa and 4 MPa m(1/2), respectively. Flexural strength of B6O-TaB2 ceramics increased up to 800 C-omicron and remained unchanged up to 1600 C-omicron. At 1800 C-omicron a rapid decrease in strength down to 300 MPa was observed and was accompanied by change in fracture mechanisms suggestive of decomposition of boron suboxide grains. Fracture toughness of B6O-TaB2 composites showed a minimum at 800 C-omicron, suggestive a relaxation of thermal stresses generated from the mismatch in coefficients of thermal expansion. Flexural strength at elevated temperatures for bulk TaB2 reference sample was also investigated. Results suggest that formation of composite provides additional strengthening/toughening as in all cases flexural strength and fracture toughness of the B6O-TaB2 ceramic composite was higher than that reported for B6O monoliths. (C) 2017 Elsevier Ltd. All rights reserved.
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