Journal
CHEMICAL COMMUNICATIONS
Volume 55, Issue 59, Pages 8623-8626Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c9cc03972d
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Funding
- Office of Naval Research [N00014-16-2109]
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A strategically novel synthesis of nano-sized, asymmetrically functionalized double-decker shaped silsesquioxanes (DDSQ) is reported. Selective protection with a boronic acid affords the crucial mono-protected intermediate en route to the asymmetric products. Generation of symmetric by-products is minimized by judicious choice of base, and high recovery of recyclable starting DDSQ tetraol is achieved.
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