Journal
CHEMICAL COMMUNICATIONS
Volume 55, Issue 61, Pages 8943-8946Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c9cc04039k
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Funding
- National Natural Science Foundation [21772046]
- Natural Science Foundation of Fujian Province [2016J01064]
- Subsidized Project for Cultivating Postgraduates' Innovative Ability in Scientific Research of Huaqiao University
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An oxidative cyclization of beta,gamma-unsaturated hydrazones for the divergent assembly of pyrazolones and pyrazolines under metal-free conditions is presented. This divergent synthetic strategy was achieved by controlling the reaction atmosphere. A number of pyrazolines were obtained via 5-exo-trig cyclization when the reaction was performed under N-2. Whereas when the reaction was conducted under O-2, diverse functionalized pyrazolones were achieved via oxidative cleavage of the CC double bond.
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