Journal
CHEMICAL COMMUNICATIONS
Volume 55, Issue 64, Pages 9563-9566Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c9cc05222d
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Funding
- National Science Centre of Poland [2015/17/B/ST4/04221]
- EPSRC [EP/L011999/1, 1954826] Funding Source: UKRI
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Pure-shift NMR enhances spectral resolution, but the optimal resolution can only be obtained at the cost of acquisition time. We propose to accelerate pure-shift acquisition using optimised 'burst' non-uniform sampling schemes [I. E. Ndukwe, A. Shchukina, K. Kazimierczuk and C. P. Butts, Chem. Commun., 2016, 52, 12769] and then reconstruct the undersampled signal mathematically. Here, we focus on the reliability of this reconstruction depending on the sampling scheme and present a workflow for the sampling optimization. It is ready to be implemented in routine measurements and yields a great improvement in reconstruction of challenging cases.
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