Journal
METHODS AND PROTOCOLS
Volume 2, Issue 3, Pages -Publisher
MDPI
DOI: 10.3390/mps2030067
Keywords
flow reaction; photochemistry; bicyclic aziridine
Categories
Funding
- Fundacao para a Ciencia e a Tecnologia (FCT) [PTDC/QUI-QOR/32008/2017, UID/DTP/04138/2013]
- PESSOA [40875QJ]
- European Research Area Network
- ERANet LAC [ELAC2014/BEE-0341]
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A new home-made UV photochemical reactor (95 cm of irradiation zone) consisting of a 12 parallel quartz tubes flow reactor, PQT6 (95 cm under irradiation and an internal diameter of 0.6 cm) was assembled to perform photochemical transformations in continuous-flow. PQT6 was evaluated for the photoreaction of 1-allylpyridinium bromide (1a) to 6-allyl-6-azabicyclo[3.1.0]hex-3-en-2-ol (2a), in a continuous process. This technology provides reduced reaction times, continuous production of 2a, and a productivity of 129 mg h(-1), corresponding to 1.94 g of isolated 2a after 15 h of irradiation.
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