Journal
JOURNAL OF SEPARATION SCIENCE
Volume 40, Issue 24, Pages 4765-4772Publisher
WILEY-V C H VERLAG GMBH
DOI: 10.1002/jssc.201700947
Keywords
deep eutectic solvents; magnetic molecularly imprinted polymers; magnetic solid-phase extraction; templates
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Funding
- Basic Science Research Program through National Research Foundation of Korea (NRF) - Ministry of Education [NRF-2015R1A4A1042434]
- National Research Foundation of Korea [2015R1A4A1042434] Funding Source: Korea Institute of Science & Technology Information (KISTI), National Science & Technology Information Service (NTIS)
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Newmagnetic molecularly imprinted polymerswith two templateswere fabricated for the recognition of polysaccharides (fucoidan and alginic acid) from seaweed by magnetic solid-phase extraction, and the materials were modified by seven types of deep eutectic solvents. It was found that the deep eutectic solvents magnetic molecularly imprinted polymers showed stronger recognition and higher recoveries for fucoidan and alginic acid than magnetic molecularly imprinted polymers, and the deep eutectic solvents-4-magnetic molecularly imprinted polymers had the best effects. The practical recovery of the two polysaccharides (fucoidan and alginic acid) purified with deep eutectic solvents-4-magnetic molecular imprinted polymers in seaweed under the optimal conditions were 89.87, and 92.0%, respectively, and the actual amounts extracted were 20.6 and 18.7 mu g/g, respectively. To sum up, the developed method proved to be a novel and promising method for the recognition of complex polysaccharide samples from seaweed.
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