Journal
DALTON TRANSACTIONS
Volume 48, Issue 34, Pages 12828-12831Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c9dt02791b
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Funding
- Ministry of Science and Higher Education [IP2015 064274]
- EU European Regional Development Fund [POIR.04.04.00-00-20C6/16-00]
- Foundation for Polish Science TEAM Program
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The charge-neutral bimetallic Zn(ii)/Co(ii) tridecanuclear oxocarboxylate cluster [ZnxCo13-x(mu(4)-O)(4)(O2CPh)(18)] (x approximate to 5.6) was synthesized under anaerobic conditions by the controlled hydrolysis of an alkylzinc carboxylate [EtZn(O2CPh)] in the presence of cobalt(ii) benzoate Co(O2CPh)(2). The composition and molecular structure of the resulting aggregates were solved by a combination of elemental analysis, infrared spectroscopy and single-crystal X-ray diffraction.
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