Journal
ORGANIC CHEMISTRY FRONTIERS
Volume 6, Issue 17, Pages 3065-3070Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c9qo00748b
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Funding
- National Natural Science Foundation of China [21772168]
- Opening Fund of the Beijing National Laboratory for Molecular Sciences
- Key Foundation of Education Bureau of Hunan Province [17A208]
- Hunan 2011 Collaborative Innovation Centre of Chemical Engineering & Technology with Environmental Benignity and Effective Resource Utilization
- Project of Innovation Team of the Ministry of Education [IRT_17R90]
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A convenient Co-catalyzed three-component decarbonylative alkylative esterification of styrene derivatives with aliphatic aldehydes and iodobenzene diacetate to provide chain elongated acetates and benzoates has been developed. Readily available aliphatic aldehydes are decarbonylated into 1 degrees, 2 degrees and 3 degrees alkyl radicals for the construction of a C(sp(3))-C(sp(3)) bond via radical addition and an interconversion of Co-II-Co-III-Co-I complexes is accountable for the formation of a C(sp(3))-O bond.
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