Journal
CHEMICAL COMMUNICATIONS
Volume 55, Issue 73, Pages 10900-10903Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c9cc05687d
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Funding
- CSIR
- Department of Science and Technology (DST) [SB/FT/CS-101/2013]
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Cocrystallization of racemic dl-tartaric acid (dl-ta) and achiral isoniazid (ISN) was investigated using mechanochemistry. Neat grinding (NG) and liquid-assisted grinding (LAG) in the presence of non-polar liquids result in the formation of a conglomerate (ISN center dot d-ta/ISN center dot l-ta); whereas LAG with polar liquids yields racemic salt ISN center dot dl-ta. The effect of solvent polarity and dipole moment in mechanochemistry is discussed.
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