4.7 Article

Benchtop flow-NMR for rapid online monitoring of RAFT and free radical polymerisation in batch and continuous reactors

Journal

POLYMER CHEMISTRY
Volume 10, Issue 35, Pages 4774-4778

Publisher

ROYAL SOC CHEMISTRY
DOI: 10.1039/c9py00982e

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Funding

  1. EPSRC [EP/S000380/1]
  2. EPSRC [EP/S000380/1] Funding Source: UKRI

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A Benchtop NMR spectrometer is used for detailed monitoring of controlled and free radical polymerisations performed in batch and continuous reactors both offline and in real-time. This allows detailed kinetic analysis with unprecedented temporal resolution for reactions which reach near completion in under five minutes.

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