Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 82, Issue 8, Pages 4305-4316Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.7b00300
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Funding
- JSPS KAKENHI [16H01157, 26293004]
- Science and Technology Research Promotion Program for Agriculture, forestry, fisheries and food industry
- Asahi Glass Foundation
- Cooperative Research Program of the Network Joint Research Center for Materials and Devices
- Grants-in-Aid for Scientific Research [17K15430, 16H01157, 26460009, 17K08231, 26293004] Funding Source: KAKEN
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A novel, practical protocol for the aerobic direct C-H acetoxylation of arenes, employing a recyclable heterogeneous rhodium catalyst, is reported herein. The trifluoroacetoxylation of 2-amido-substituted anthracenes proceeded at the 9-position with exclusive regioselectivity. The oxidation of variously substituted anthracenes and other polycyclic aromatics with molecular oxygen as a terminal oxidant proceeded under mild conditions, providing products in good to excellent yields.
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