Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 82, Issue 3, Pages 1437-1447Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.6b02614
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Funding
- National Research Foundation of Korea (NRF) grants - Korean government (MSIP) [2011-0018355, 2015111C1A1035955]
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A method for the synthesis of a wide range of fused thiophenes, including those fused with lactams, lactones, or cyclic ethers, was developed from a rhodium-catalyzed intramolecular transannulation reaction of alkynyl thiadiazoles. This transannulation reaction provides an efficient platform for the construction of a variety of 5,n-fused thiophenes from readily available starting materials together with the release of molecular nitrogen.
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