Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 82, Issue 13, Pages 7015-7022Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.7b00907
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Funding
- National Natural Science Foundation of China [21372137, 21572110]
- Natural Science Foundation of Shandong Province [ZR2014BM006]
- Science and Technology Development Project in University of Shandong Province [J16LC12]
- Applied Basic Research Project (Youth Special) of Qingdao [16-5-1-98-jch]
- Research Fund of State Key Laboratory for Marine Corrosion and Protection of Luoyang Ship Material Research Institute [KF160404]
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A novel Mn(II)-promoted tandem phosphorylation/cyclization reaction of 2-biaryl isothiocyanates with phosphine oxides is described. This is the first general method to synthesize 6-phosporylated phenanthridines from 2-Diaryl isothiocyanates. The approach is featured by oxidant-free, low loading of P-reagent, easy operation, and high functional group tolerance.
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