Journal
JOURNAL OF ORGANIC CHEMISTRY
Volume 82, Issue 12, Pages 6192-6201Publisher
AMER CHEMICAL SOC
DOI: 10.1021/acs.joc.7b00755
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Funding
- Chinese University of Hong Kong Start-up Fund, Faculty Strategic Development Funding
- Direct Grant for Research [4053199]
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A domino hydroboration/trifluoromethylation (formal hydrotrifluoromethylation) of alkynes using the fluoroform-derived [CuCF3] reagent is achieved. Synthetically useful (E)-alkenyl-CF3 building blocks and 1,1-bis(trifluoromethyl)-substituted alkenes can be prepared under ambient conditions in one pot/one step from alkynes. The ultimate source of CF3 is the inexpensive industrial waste fluoroform.
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