Journal
REACTION CHEMISTRY & ENGINEERING
Volume 4, Issue 12, Pages 2055-2059Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c9re00265k
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Herein, we report a highly selective preparation method of azoxybenzenes from nitrobenzenes by visible-light irradiation. In a batch, this reaction method affords the corresponding aniline derivatives or intermediates (nitrosobenzene or phenyl hydroxylamine); however, in flow microreactors, azoxybenzenes are successfully obtained with very high selectivity.
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