Journal
CHEMICAL COMMUNICATIONS
Volume 55, Issue 96, Pages 14426-14429Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c9cc08229h
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Funding
- U.S. Department of Energy, Office of Science, Office of Basic Energy Sciences, Catalysis Science program [DE-SC0019179]
- ACS Green Chemistry Pharmaceutical Roundtable [2016]
- ACS Petroleum Research Fund [59542-ND1]
- U.S. Department of Energy (DOE) [DE-SC0019179] Funding Source: U.S. Department of Energy (DOE)
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Herein we report the development of diffusion ordered NMR spectroscopy (DOSY) for its use to characterize metal complexes containing paramagnetic first row transition metal elements. This technique is capable of assessing the purity and speciation of paramagnetic complexes, and also provides a convenient method to provide qualitative and sometimes quantitative molecular weight data.
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