Journal
CATALYSIS SCIENCE & TECHNOLOGY
Volume 10, Issue 1, Pages 105-112Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c9cy01303b
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- U.S Department of Energy's Advanced Research Project Agency Energy (ARPA-E) Renewable Energy to Fuels Through Utilization of Energy-Dense Liquids (REFUEL) program [DE-AR-0000811]
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Nanostructured catalysts for low-temperature ammonia synthesis have been developed via thermal treatment under nitrogen of Ru-containing MOFs. The resulting catalysts reveal high concentration of small Ru nanocrystals (<4 nm) well-dispersed on a graphitic carbon shell demonstrating stable ammonia formation rates at low temperature. Additional acetylene pre-treatment leads to more dispersed active catalysts containing stable sub-nanometric Ru clusters.
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