Journal
CHEMICAL COMMUNICATIONS
Volume 56, Issue 11, Pages 1713-1716Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/c9cc09276e
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Funding
- China Scholarship Council (CSC)
- ANR [ANR-17-CE07-0050]
- Universite Paris Sud
- CNRS
- Agence Nationale de la Recherche (ANR) [ANR-17-CE07-0050] Funding Source: Agence Nationale de la Recherche (ANR)
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We report an efficient and environmentally friendly electrochemical approach to perform the bromo cyclization of tryptophol, tryptamine and tryptophan derivatives. The 3a-bromofuranoindolines and 3a-bromopyrroloindolines obtained are of interest in the total synthesis of natural products. This dearomative procedure relies on the generation of an electrophilic bromine reagent by the electrochemical oxidation of MgBr2. No organic byproducts are generated with this protocol which avoids the use of an additional electrolyte.
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