4.6 Article

Synthesis of ZIF-11 crystals by microwave heating

Journal

NEW JOURNAL OF CHEMISTRY
Volume 44, Issue 9, Pages 3562-3565

Publisher

ROYAL SOC CHEMISTRY
DOI: 10.1039/c9nj04589a

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Funding

  1. National Science Foundation NSF-CBET Award [1705675]
  2. Directorate For Engineering
  3. Div Of Chem, Bioeng, Env, & Transp Sys [1705675] Funding Source: National Science Foundation

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We demonstrate the synthesis of zeolitic imidazolate framework ZIF-11 via a microwave assisted approach. The resultant 2-7 mu m crystals were synthesized in minutes and displayed BET surface areas as high as 745 m(2) g(-1). The state-of-the-art ZIF-11 synthesis techniques are summarized. XRD, SEM, and porosimetry were used as pivotal characterization techniques.

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