Journal
ORGANIC & BIOMOLECULAR CHEMISTRY
Volume 18, Issue 8, Pages 1567-1571Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/d0ob00189a
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Funding
- Carl-Zeiss Foundation
- Friedrich Schiller University Jena
- DAAD
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P-Rhodamines were accessed by implementing a robust three step sequence consisting of (i) addition of m-metallated anilines to dichlorophosphine oxides, (ii) selective dibromination, and (iii) cyclization of the diaryllithium reagents derived from the dibromides to form the dihydroacridophosphine core of P-rhodamines. A modified route was developed to produce non-symmetric P-rhodamines. A library of prepared P-rhodamines provides first insight into dependence of fluorophore properties on the structure of P-rhodamines. A P-rhodamine with highest batochromic shifts and quantum yields in the class was identified.
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