Journal
CHEMICAL COMMUNICATIONS
Volume 56, Issue 33, Pages 4535-4538Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/d0cc01356k
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Funding
- Office of Science, Office of Basic Energy Sciences, Division of Chemical Sciences, Geosciences, and Biosciences Heavy Element Chemistry Program of the U.S. Department of Energy (DOE) at LBNL [DE-AC02-05CH11231]
- NSF GRFP [DGE 1106400]
- NIH [1R35GM126961-01, S10OD024998]
- Daimler and Benz Foundation [32-06/17]
- Fonds der chemischen Industrie (VCI)
- Paderborn University
- University of Innsbruck
- Office of Science, Office of Basic Energy Sciences, of the U.S. DOE [DE-AC02-05CH11231]
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Reaction of (Cp-iPr4)(2)UI with NaN3 resulted in formation of tetrameric uranium(iii) azide-bridged 'molecular square' [(Cp-iPr4)(2)U(mu-eta(1):eta(1)-N-3)](4) (1). Addition of B(C6F5)(3) to 1 induced loss of N-2 at room temperature, yielding the uranium(v) borane-capped nitrido (Cp-iPr4)(2)U(mu-N)B(C6F5)(3) (2).
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