Journal
NANOSCALE ADVANCES
Volume 2, Issue 6, Pages 2347-2351Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/d0na00153h
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Funding
- Engineering and Physical Sciences Research Council (EPRSC) UK [EP/L015544]
- UoB
- EPSRC [EP/K035746/1, EP/M028216/1]
- EPSRC [EP/K035746/1, EP/L022532/1, EP/M028216/1] Funding Source: UKRI
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We investigate the phase-transition behaviour of nickel nanoparticles (3-6 nm)viadynamic TEM. The nanoparticles were synthesized within a reverse microemulsion and then monitoredviadynamic TEM simultaneously while undergoing controlled heating. The size-dependent melting point depression experimentally observed is compared with, and is in good agreement with existing thermodynamic and molecular dynamic predictions.
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