Journal
ORGANIC CHEMISTRY FRONTIERS
Volume 7, Issue 15, Pages 2075-2081Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/d0qo00601g
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Funding
- National Natural Science Foundation of China [21572051, 21602057, 21901071, 21971061]
- Natural Science Foundation of Hunan Province [2020JJ5350, 2020JJ5347]
- Scientific Research Fund of Hunan Provincial Education Department [18A002, 19B359]
- Science and Technology Planning Project of Hunan Province [2018TP1017]
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A palladium-catalyzed three-component tandem reaction for stereoselective assembly of various tri- or tetrasubstituted vinylsilanes is established. This method enables the construction of two C-Si bonds and two C-C bonds by the disilylation ofortho-vinyl bromobenzenes generatedin situfrom 1-bromo-2-iodobenzenes andN-tosylhydrazones. More importantly, the substrate scope of this protocol was further demonstrated by the transformation ofortho-vinyl bromobenzenes generated from a range of aryl iodides andN-tosylhydrazone to vinylsilanes.
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