3.8 Article

Understanding the Hot Working Behavior of a Ni-Base Superalloy XH 67 via Processing Map Approach

Journal

MATERIALS PERFORMANCE AND CHARACTERIZATION
Volume 9, Issue 2, Pages 224-236

Publisher

AMER SOC TESTING MATERIALS
DOI: 10.1520/MPC20190110

Keywords

hot working; Ni-base superalloys; discontinuous dynamic recrystallization; processing map; kinetic analysis

Funding

  1. Indian Space Research Organization (ISRO) -Indian Institute of Technology Madras (IITM) [ISRO-IITM/MET/14-15/153/ISRO/KRAV]
  2. Department of Science and Technology (DST), Government of India [SR/FST/ETII-049]

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Hot deformation behavior of nickel-based superalloy XH 67 (Ni-18.5Cr-4.5Mo-4.5W-3.0Fe-2.5Ti-1.2Al) was investigated in the temperature range of 900 degrees C-1,200 degrees C and in the strain rate range of 10(-3)-10 s(-1). A processing map was generated from the flow stress data. Detailed postdeformation microscopy was carried out to understand the microstructural evolution during hot deformation. Correlation of the kinetic analysis together with microstructural characterization studies was accomplished to identify the rate controlling mechanism. An increase in the fraction of Sigma 3 boundaries is observed with an increase in the strain rate at 1,150 degrees C. In the temperature range of 1,100 degrees C-1,200 degrees C, discontinued dynamic recrystallization has been identified as the major softening mechanism. Based on the critical analysis of the mechanical data together with microstructural analysis, the safe hot working regime for the XH 67 alloy is established to have a temperature range of 1,100 degrees C-1,200 degrees C and a strain rate range of 10(-3) to 5 x10(-2) s(-1).

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