Journal
RSC ADVANCES
Volume 10, Issue 47, Pages 28100-28105Publisher
ROYAL SOC CHEMISTRY
DOI: 10.1039/d0ra03800h
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Funding
- National Natural Science Foundation of China [21978066, 21506046]
- Basic Research Program of Hebei Province for Natural Science Foundation
- Key Basic Research Project [18964308D]
- Natural Science Foundation of Hebei Province [B2018202220]
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A novel silica-immobilized nickel and acid ionic liquid (Ni-IL/SiO2) catalyst was prepared by combining a bonding procedure with an impregnation operation and was characterized by means of X-ray diffraction (XRD), Fourier transform infrared (FT-IR) spectra, X-ray photoelectron spectroscopy (XPS) and thermogravimetric analysis (TGA) techniques. Its catalytic performance was evaluated for the one-pot synthesis of 2-propylheptanol (2-PH)viaa sequentialn-valeraldehyde self-condensation and hydrogenation reaction. As a result, Ni-IL/SiO(2)showed an excellent catalytic activity for the one-pot synthesis of 2-PH, affording a 2-PH selectivity of 75.4% at an-valeraldehyde conversion of 100% and the sum of 2-PH and pentanol selectivity reached 98.6% under the suitable reaction conditions.
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